Synthesis and crystal structure of 1-Benzenesulfonyl-4-benzhydryl-piperazine

Ananda Kumar, C. S. and Benaka Prasad, S. B. and Thimmegowda, N. R. and Rangappa, K. S. and Chandrappa, S. and Naveen, S. and Sridhar, M. A. and Shashidhara Prasad, J. (2007) Synthesis and crystal structure of 1-Benzenesulfonyl-4-benzhydryl-piperazine. Molecular Crystals and Liquid Crystals, 469 (1). pp. 111-119. ISSN 1563-5287

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Abstract

1-Benzenesulfonyl-4-benzhydryl-piperazine was synthesized from 1-benzhydryl piperazine with benzenesulfonyl chloride. The title compound, C23H24N2O2S, was synthesized and the structure was investigated by X-ray crystallography. The compound crystallizes in the monoclinic crystal class in the space group P21/c with cell parameters a = 13.2390(10) Å, b = 9.1960(7) Å, c = 18.5810(16) Å, β = 110.873(3)°, and Z = 4. The piperazine ring in the structure is in a chair conformation. The geometry around the S atom is distorted tetrahedral. The structure exhibits an intermolecular hydrogen bond of the type C‒H · O.

Item Type:	Article
Subjects:	C Chemical Science > Chemistry
Divisions:	Department of > Chemistry
Depositing User:	C Swapna Library Assistant
Date Deposited:	24 Sep 2019 05:48
Last Modified:	24 Sep 2019 05:48
URI:	http://eprints.uni-mysore.ac.in/id/eprint/8428

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