Saberi, Ali and Manjunath, H. R. and Naveen, S. and Mahadeva Prasad, T. N. and Rangappa, K. S. and Sridhar, M. A. and Shashidhara Prasad, J. (2009) Microwave-assisted synthesis and crystal structure of 1-(4-chlorophenyl)-4,5-diphenyl-2-(3,4,5-trimethoxyphenyl)-1h-imidazole. Molecular Crystals and Liquid Crystals, 515. pp. 199-206. ISSN 1563-5287
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The title compound, 1-(4-chlorophenyl)-4,5-diphenyl-2-(3,4,5-trimethoxy-phenyl)-1H-imidazole , was synthesized using a domestic microwave oven, and the structure of the product obtained was confirmed by X-ray diffraction (XRD) studies. The compound, C30H25ClN2O3, crystallizes in the triclinic crystal class in the space group image omitted] with cell parameters a=10.635(15) angstrom, b=12.262(2) angstrom, c=11.656(3) angstrom, =69.817(15)degrees, =64.630(6)degrees, =73.503(16)degrees, and Z=2. The structure has been solved by direct methods and refined to R1=0.0764 for 3078 unique reflections with I2 sigma(I). The imidazole ring in the structure adopts a planar conformation. No classic hydrogen bonds were found in the structure.
| Item Type: | Article |
|---|---|
| Uncontrolled Keywords: | crystal structure; equatorial confirmation; imidazole ring; microwave oven |
| Subjects: | C Chemical Science > Chemistry D Physical Science > Physics |
| Divisions: | Department of > Chemistry Department of > Physics |
| Depositing User: | Users 19 not found. |
| Date Deposited: | 30 Aug 2019 06:22 |
| Last Modified: | 30 Aug 2019 06:22 |
| URI: | http://eprints.uni-mysore.ac.in/id/eprint/7369 |
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