Mahesh, M. J. and Gopalakrishna, G. S. and Ashamanjari (2006) Pre-treated and treated hydrothermal preparation of NaVP2O7·H2O crystalline material and its characterization. Materials Characterization, 57 (1). 30 - 35. ISSN 1873-4189
Full text not available from this repository. (Request a copy)Abstract
NaVP2O7·H2O crystalline material was synthesized by a hydrothermal technique at moderate P–T condition. The resultant material was characterized by SEM, powder XRD, DTA, FTIR and magnetic susceptibility studies. Powder X-ray studies revealed that the NaVP2O7·H2O compound has crystallized in monoclinic system with cell parameters a=22.1737, b=8.0520, c=11.4670 Å, β=103.751, V=1988.66 Å3. Repetitive hydrothermal treatment of the material yielded improved size and quality of crystals. Magnetically this material is paramagnetic; however the μeff decreased as the size of the crystals increased.
| Item Type: | Article |
|---|---|
| Uncontrolled Keywords: | Hydrothermal synthesis, Vanadium phosphate, XRD, DTA, FT-IR, Paramagnetic |
| Subjects: | F Earth Science > Geology |
| Divisions: | Department of > Earth Science |
| Depositing User: | LA manjunath user |
| Date Deposited: | 17 Aug 2019 10:46 |
| Last Modified: | 17 Aug 2019 10:46 |
| URI: | http://eprints.uni-mysore.ac.in/id/eprint/6698 |
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