Lakshminarayana, B. N. and Gnanendra, C. R. and Mahadeva Prasad, T. N. and Sridhar, M. A. and Naik, Nagaraja and Chenne Gowda, D. and Shashidhara Prasad, J. (2010) Structural Conformation of a Novel Piperidine-4-One Derivative: 1-Acryloyl-3-Methyl-2,6-Dip-Tolylpiperidine-4-One. Journal of Chemical Crystallography, 40 (8). pp. 686-690. ISSN 1074-1542
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Abstract
The novel 3-methyl-2,6-dip-toylpiperidine-4-one was acylated by 3-chloropropanoychloride and subjected for dehydrohalogenation. The synthesized compound was characterized by spectroscopic techniques and finally confirmed by X-ray diffraction studies. The molecule crystallizes in the monoclinic crystal class in the space group C2/c with cell parameters a = 18.538(2) Å, b = 9.9050(1) Å, c = 22.954(2) Å, β = 94.486(8)° and Z = 8. The piperidine ring adopts a twist boat conformation.
Item Type: | Article |
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Subjects: | C Chemical Science > Chemistry |
Divisions: | Department of > Chemistry |
Depositing User: | LA manjunath user |
Date Deposited: | 09 Jul 2019 05:21 |
Last Modified: | 11 Dec 2019 09:15 |
URI: | http://eprints.uni-mysore.ac.in/id/eprint/4949 |
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