Amrutha Kala, A. L. and Karthik Kumara, . and Pavithra, G. and Ajay Kumar, K. and Lokanath, N. K. (2017) Crystal structure and Hirshfeld surface analysis of (E)-2-(1-(2-phenylhydrazono)ethyl)naphtholen-1-ol. Chemical Data Collections, 7-8. 107 - 115. ISSN 2405-8300
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The Schiff base analogue (E)-2-(1-(2-phenyl hydrazono)ethyl)naphtholen-1-ol was synthesized by condensation reaction of 2-acetyl-1-hydroxynaphthol and phenylhydrazine hydrochloride in the presence of sodium acetate in ethyl alcohol under reflux conditions. The product obtained was characterized by 1H NMR, MS and single crystal X-ray diffraction studies. The compound crystallizes in the monoclinic crystal system with space group C2/c and unit cell parameters, a = 17.69(3) Å, b = 7.885(15) Å, c = 21.97(5) Å and β = 108.36(3)° and Z = 8. The molecular structure exhibits intra-molecular hydrogen bonds C—H…N, O—H…N and C— H…π, π- π intermolecular interactions.
| Item Type: | Article |
|---|---|
| Uncontrolled Keywords: | Schiff base, Condensation, X-ray diffraction, Crystal structure, Interactions |
| Subjects: | C Chemical Science > Chemistry |
| Divisions: | Yuvaraj college > Chemistry |
| Depositing User: | C Swapna Library Assistant |
| Date Deposited: | 14 Jun 2019 06:08 |
| Last Modified: | 18 Jul 2022 05:30 |
| URI: | http://eprints.uni-mysore.ac.in/id/eprint/3043 |
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