Structural Conformation of a Novel Piperidine-4-One Derivative: 1-Acryloyl-3-Methyl-2,6-Dip-Tolylpiperidine-4-One

Lakshminarayana, B. N. and Gnanendra, C. R. and Mahadeva Prasad, T. N. and Sridhar, M. A. and Naik, Nagaraja and Chenne Gowda, D. and Shashidhara Prasad, J. (2010) Structural Conformation of a Novel Piperidine-4-One Derivative: 1-Acryloyl-3-Methyl-2,6-Dip-Tolylpiperidine-4-One. Journal of Chemical Crystallography, 40 (8). pp. 686-690. ISSN 1074-1542

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The novel 3-methyl-2,6-dip-toylpiperidine-4-one was acylated by 3-chloropropanoychloride and subjected for dehydrohalogenation. The synthesized compound was characterized by spectroscopic techniques and finally confirmed by X-ray diffraction studies. The molecule crystallizes in the monoclinic crystal class in the space group C2/c with cell parameters a = 18.538(2) Å, b = 9.9050(1) Å, c = 22.954(2) Å, β = 94.486(8)° and Z = 8. The piperidine ring adopts a twist boat conformation.

Item Type: Article
Subjects: C Chemical Science > Chemistry
Divisions: Department of > Chemistry
Depositing User: LA manjunath user
Date Deposited: 09 Jul 2019 05:21
Last Modified: 11 Dec 2019 09:15

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