Crystal structure and Hirshfeld surface analysis of (E)-2-(1-(2-phenylhydrazono)ethyl)naphtholen-1-ol

Amrutha Kala, A. L. and Kumara, Karthik and Pavithra, G. and Ajay Kumar, K. and Lokanath, N. K. (2017) Crystal structure and Hirshfeld surface analysis of (E)-2-(1-(2-phenylhydrazono)ethyl)naphtholen-1-ol. Chemical Data Collections, 7-8. 107 - 115. ISSN 2405-8300

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The Schiff base analogue (E)-2-(1-(2-phenyl hydrazono)ethyl)naphtholen-1-ol was synthesized by condensation reaction of 2-acetyl-1-hydroxynaphthol and phenylhydrazine hydrochloride in the presence of sodium acetate in ethyl alcohol under reflux conditions. The product obtained was characterized by 1H NMR, MS and single crystal X-ray diffraction studies. The compound crystallizes in the monoclinic crystal system with space group C2/c and unit cell parameters, a = 17.69(3) Å, b = 7.885(15) Å, c = 21.97(5) Å and β = 108.36(3)° and Z = 8. The molecular structure exhibits intra-molecular hydrogen bonds C—H…N, O—H…N and C— H…π, π- π intermolecular interactions.

Item Type: Article
Uncontrolled Keywords: Schiff base, Condensation, X-ray diffraction, Crystal structure, Interactions
Subjects: C Chemical Science > Chemistry
Divisions: Yuvaraj college > Chemistry
Depositing User: MUL SWAPNA user
Date Deposited: 14 Jun 2019 06:08
Last Modified: 14 Jun 2019 06:08

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