A comparative study of microwave versus conventional synthesis of lead phthalocyanine complexes

Narayana Achar, B. and Mohan Kumar, T. M. and Lokesh, K. S. (2005) A comparative study of microwave versus conventional synthesis of lead phthalocyanine complexes. Journal of Porphyrins and Phthalocyanines, 09 (12). pp. 872-879. ISSN 1099-1409

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Official URL: https://doi.org/10.1142/S1088424605001003

Abstract

Lead(II) phthalocyanine (PbPc); lead(II) tetranitrophthalocyanine (PbTNP) and lead(II) tetraaminophthalocyanine (PbTAP) were synthesized in pure state by microwave irradiation and conventional heating methods. The procedures for their synthesis by the microwave technique are standardized and reported for the first time. PbPc and PbTNP were synthesized in dry conditions and PbTAP complex was synthesized in aqueous medium. All the compounds are obtained in very high yield (~90%). The synthesized complexes are characterized with respect to elemental analysis, UV-visible, IR-spectroscopy and X-ray diffraction study. The microwave methods are advantageous over the conventional method of synthesis with respect to higher yield, rapidity and simplicity.

Item Type: Article
Subjects: C Chemical Science > Chemistry
Divisions: Department of > Chemistry
Depositing User: manjula User
Date Deposited: 09 Sep 2019 10:30
Last Modified: 09 Sep 2019 10:30
URI: http://eprints.uni-mysore.ac.in/id/eprint/7874

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