Redetermination of N,N′-bis­­(4-chloro­phenyl)­thio­urea at 173 K

Sarojini, B. K. and Narayana, B. and Swamy, M. T. and Yathirajan, H. S. and Bolte, Michael (2007) Redetermination of N,N′-bis­­(4-chloro­phenyl)­thio­urea at 173 K. Acta Crystallographica Section E, 63 (9). o3879. ISSN 2056-9890

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Abstract

The structure of the title compound, C13H10Cl2N2S, has already been determined at room temperature [Soriano-García, Chávez, Cedillo, Pérez & Hernández (2001[Soriano-García, M., Chávez, G. T., Cedillo, F. D., Pérez, A. E. D. & Hernández, G. A. (2001). Anal. Sci. 17, 799-800.]). Anal. Sci. 17, 799–800]. However, the positions of the H atoms were not provided. Thus, we present here the complete structure determined from data at low temperature (173 K). The mol­ecules are connected via bifurcated N—H⋯S hydrogen bonds to form zigzag chains running along the b axis. The title compound is isomorphous with 1,3-bis­(4-bromo­phen­yl)thio­urea.

Item Type:	Article
Subjects:	C Chemical Science > Chemistry
Divisions:	Department of > Chemistry
Depositing User:	C Swapna Library Assistant
Date Deposited:	09 Sep 2019 09:56
Last Modified:	09 Sep 2019 09:56
URI:	http://eprints.uni-mysore.ac.in/id/eprint/7861

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