Synthesis and crystal structure of Tert-butyl 2-((phenylthio)-carbonyl)pyrrolidine-1-carboxylate

Naveen, S. and Dinesh, B. and Abiraj, K. and Channe Gowda, D. and Sridhar, M. A. and Shashidhara Prasad, J. (2007) Synthesis and crystal structure of Tert-butyl 2-((phenylthio)-carbonyl)pyrrolidine-1-carboxylate. Journal of Chemical Crystallography, 37 (11). pp. 721-725. ISSN 1572-8854

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Tert-butyl 2-((phenylthio)carbonyl)pyrrolidine-1-carboxylate, was synthesized by using iso-butoxycarbonyl chloride (i-BuOCOCl) via mixed anhydride method. The obtained product was characterized spectroscopically and finally confirmed by X-ray diffraction studies. The title compound C16 H21 N O3 S crystallizes in the triclinic space group P1 with the cell parameters a = 6.0250(7) Å, b = 8.2820(13) Å, c = 8.7700(14) Å, α = 102.352(4)°, β = 102.993(11)°, γ = 90.279(8)°, V = 415.89(10) Å3 and Z = 1. The proline ring in the structure is in a envelope conformation. The structure exhibits intermolecular hydrogen bonds of the type C--H...O.

Item Type: Article
Subjects: D Physical Science > Physics
Divisions: Department of > Physics
Depositing User: C Swapna Library Assistant
Date Deposited: 07 Sep 2019 05:20
Last Modified: 23 Jun 2022 10:44

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