Hydrothermal synthesis and characterization of CsNiP and 2(LiZnHP2O7) crystals

Gopalakrshna, G. S. and Mahesh, M. J. and Madhu, S. P. and Ashamanjari, K. G. and Shridhara, M. A. and Prasad, S. (2006) Hydrothermal synthesis and characterization of CsNiP and 2(LiZnHP2O7) crystals. Journal of Materials Science, 41 (5). pp. 1423-1427. ISSN 1573-4803

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Official URL: https://doi.org/10.1007/s10853-006-7443-5


CsNiP and 2(LiZnHP2O7) crystals were synthesized by hydrothermal technique at moderate P-T conditions. Solubility results of both the compound shown positive thermal coefficient and single crystal X-ray studies revealed, CsNiP crystallized in hexagonal system with cell parameters; a = 7.173(2), c = 5.944(9) Å, V = 264.87(7) Å3 and space group P63/mmc and 2(LiZnHP2O7) crystallized in orthorhombic system with cell parameters; a = 12.3636 Å, b = 27.5330 Å, c = 6.8647 Å and space group, Pca21 exhibiting ring type of cavities with open aperture in the structure. CsNiP is a frequency dependent paramagnetic and 2(LiZnHP2O7) is a diamagnetic.

Item Type: Article
Subjects: F Earth Science > Geology
Divisions: Department of > Earth Science
Depositing User: LA manjunath user
Date Deposited: 27 Aug 2019 06:52
Last Modified: 27 Aug 2019 06:52
URI: http://eprints.uni-mysore.ac.in/id/eprint/7120

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