Naveen, S. and Ananda Kumar, C. S. and Benaka Prasad, S. B. and Vinaya, K. and Sridhar, M. A. and Shashidhara Prasad, J. and Rangappa, K. S. (2009) Structural conformation of a novel 1-benzhydrylpiperazine derivative: 1-benzhydryl-4-(toluene-4-sulfonyl)-piperazine. Journal of Chemical Crystallography, 39 (6). pp. 395-398. ISSN 1572-8854
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The title compound 1-benzhydryl-4-(toluene-4-sulfonyl)-piperazine was synthesized and the structure was investigated by X-ray crystallography. The title compound, C24H26N2O2S crystallizes in the monoclinic crystal class in the space group P2(1)/c with cell parameters a = 13.5800(10) angstrom, b = 8.9630(7) angstrom, c = 18.9040(10) angstrom, beta = 106.851(3)degrees, Z = 4 and V = 2202.1(3) angstrom(3). The structure has been solved by direct methods and refined to R-1 = 0.0468 for 3174 observed reflections I > 2 sigma(I). The structure reveals that the piperazine ring is in a chair conformation. The geometry around the S atom is a distorted tetrahedron.
Item Type: | Article |
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Uncontrolled Keywords: | Benzhydrylpiperazine; Sulfonyl chloride; Crystal structure; Tetrahedral configuration |
Subjects: | C Chemical Science > Chemistry D Physical Science > Physics |
Divisions: | Department of > Chemistry Department of > Physics |
Depositing User: | Users 19 not found. |
Date Deposited: | 26 Aug 2019 05:50 |
Last Modified: | 26 Aug 2019 05:50 |
URI: | http://eprints.uni-mysore.ac.in/id/eprint/7006 |
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