Synthesis, characterization, crystal structure and Hirshfeld surface analysis of o-tolyloxy acetic acid (1H-indol-3-yl-methylene)-hydrazide

Mamatha, S. V. and Naveen, S. and Zabiulla and Mohammed, Yasser H. E. and Lokanath, N. K. and Khanum, Shaukath Ara (2017) Synthesis, characterization, crystal structure and Hirshfeld surface analysis of o-tolyloxy acetic acid (1H-indol-3-yl-methylene)-hydrazide. Chemical Data Collections, 11-12. 1 - 10. ISSN 2405-8300

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Official URL: https://doi.org/10.1016/j.cdc.2017.07.003

Abstract

o-Tolyloxy acetic acid (1H-indol-3-yl-methylene)-hydrazide was synthesized by treating 2-methyl phenoxy acetic acid hydrazide with indole carboxaldehyde. It was characterized by NMR, IR studies and mass spectral studies and finally, the structure was confirmed by single crystal X-ray diffraction studies. The title compound C18H17N3O2 crystallizes in the monoclinic crystal system in the space group P21/n. The intermolecular interactions in the crystal structures are quantified using the Hirshfeld surface analysis method. The majority contribution to the Hirshfeld surfaces is from H⋯H (45.4) contacts.

Item Type: Article
Uncontrolled Keywords: Indole, o-Tolyloxy acetic acid (1H-indol-3-yl-methylene)-hydrazide, X-ray diffraction, Hirshfeld surface analysis
Subjects: ?? QC ??
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Divisions: Department of > Chemistry
Department of > Physics
Depositing User: C Swapna Library Assistant
Date Deposited: 29 May 2019 05:54
Last Modified: 28 Jun 2019 09:31
URI: http://eprints.uni-mysore.ac.in/id/eprint/608

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