Synthesis, characterization, and crystal structure of (E)-1-(4-(1-Isobutyl-1 H-imidazo 4, 5-c quinolin-4-ylamino) phenyl)-3-phenylprop-2-en-1-one

Prabhuswamy, M. and Dinesha and Pampa, K. J. and Nagaraja, G. K. and Lokanath, N. K. (2015) Synthesis, characterization, and crystal structure of (E)-1-(4-(1-Isobutyl-1 H-imidazo 4, 5-c quinolin-4-ylamino) phenyl)-3-phenylprop-2-en-1-one. Molecular Crystals and Liquid Crystals, 623 (1). pp. 253-264. ISSN 1563-5287

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Abstract

(E)-1-(4-(1-Isobutyl-1H-imidazo[4,5-c]quinolin-4-ylamino)phenyl)-3-phenylprop-2- en-1-one, C29H26N4O, was synthesized and characterized by spectroscopy and elemental analysis. The crystal structure was determined from single crystal X-ray diffraction data. It crystallizes in the triclinic crystal system with the space group P¯ı, and unit cell parameters, a = 9.667(2) Å, b = 11.408(3) Å, c = 12.286(3) Å, α = 116.7(1)◦, β = 91.5(1)◦, γ = 99.6(1)◦, Z = 2, CuKα = 1.5418 Å, and final R1 and wR2 being 0.067 and 0.189, respectively. The molecular and crystal structures of the title molecule are stabilized by intramolecular interactions, N—H···N, C—H···N, and C—H···O, and intermolecular interaction, CH···O.

Item Type:	Article
Subjects:	B Life Science > Microbiology C Chemical Science > Chemistry D Physical Science > Physics
Divisions:	Department of > Chemistry Department of > Microbiology Department of > Physics
Depositing User:	Users 19 not found.
Date Deposited:	27 May 2019 10:56
Last Modified:	17 Sep 2019 09:58
URI:	http://eprints.uni-mysore.ac.in/id/eprint/578

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