Synthesis characterization and crystal structure of 2-(3,4,5- trimethoxyphenyl)-1-(4-fluorophenyl)-4,5-diphenyl-1H-imidazole

Viveka, S. and Prabhuswamy, M. and Dinesha and Lokanath, N. K. and Nagaraja, G. K. (2014) Synthesis characterization and crystal structure of 2-(3,4,5- trimethoxyphenyl)-1-(4-fluorophenyl)-4,5-diphenyl-1H-imidazole. Molecular Crystals and Liquid Crystals, 593 (1). pp. 261-270. ISSN 1542-1406

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The title compound, C30H25FN2O3, was prepared from the four-component one-pot condensation reaction and the product crystallized using dimethylformamide. The structure of the compound was established by elemental analysis, Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), UV-Visible, and single-crystal X-ray diffraction. The compound crystallizes in the triclinic crystal system with the space group Pī, with unit cell parameters a = 10.286(2) Å, b = 11.795(2) Å, c = 21.331(4) Å, α = 100.270(3)°, β = 90.093(3)°, γ = 90.062(3)°, and Z = 4. The crystal and molecular structure of the title molecule is stabilized by intra-molecular interactions of types C–H···N and C–H···O.

Item Type: Article
Uncontrolled Keywords: Crystal structure, X ray diffraction, Fourier transform infrared spectroscopy, Thermogravimetric analysis, Condensation reactions, Intermolecular interactions, Molecular structure, FT-IR spectrum, Crystallization, Multi-component reactions, Imidazole, Thermo gram
Subjects: D Physical Science > Physics
Divisions: Department of > Physics
Depositing User: Arshiya Kousar Library Assistant
Date Deposited: 03 Jul 2019 05:31
Last Modified: 03 Jul 2019 05:31

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