Synthesis, crystal structure and characterization of (Z)-2-N′- hydroxyisonicotinamidine

Prabhuswamy, M. and Dinesha and Pampa, K. J. and Madan Kumar, S. and Nagaraja, G. K. and Lokanath, N. K. (2014) Synthesis, crystal structure and characterization of (Z)-2-N′- hydroxyisonicotinamidine. Molecular Crystals and Liquid Crystals, 593 (1). pp. 243-252. ISSN 1563-5287

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The compound (Z)-2-N′-hydroxyisonicotinamidine, (2) was synthesized and characterized by 1H NMR, FT-IR, FAB-Mass, UV-Visible Spectra, and elemental Analysis. Its molecular structure was solved by single crystal X-ray diffraction method. The title molecule, C6H7N3O is crystallized in the orthorhombic crystal system with the space group Pna2 1 and with unit cell parameters a = 12.5664(8) à , b = 8.8622(6) à , c = 5.7953(4) A, α = 90°, β; = 90°, γ = 90°, and Z = 4. The molecular and crystal structure of the title molecule is stabilized by an intramolecular interaction of the type N.HEEEO, and the intermolecular interactions of types N—H•••N and O—H•••N.

Item Type: Article
Uncontrolled Keywords: Crystal structure, Single crystal X-ray diffraction method, Single crystals, Molecules, X ray diffraction, Intermolecular interactions, Intramolecular interactions, Molecular structure, Characterization, Amidoxime, Space Groups, Orthorhombic crystal system, Unit cell parameters, UV-Visible spectra
Subjects: B Life Science > Microbiology
D Physical Science > Physics
Divisions: Department of > Microbiology
Department of > Physics
Depositing User: Arshiya Kousar Library Assistant
Date Deposited: 22 Aug 2019 05:45
Last Modified: 22 Aug 2019 05:48

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