Bhat, Mahesh and Belagali, S. L. and Madan Kumar, S. and Byrappa, K. (2017) Synthesis, characterization and crystal structure of 4-(6-ethoxy benzothiazol-2-yl) diazenyl phenyl 2-(2, 3-dihydro-1H-inden-2-yl) acetate. Chemical Data Collections, 7-8. 1 - 7. ISSN 2405-8300
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The title compound C26H23N3O3S was synthesized by Steglich esterification of 4-(6-ethoxy benzothiazol-2-yl) diazenyl phenol with Indan-2-ylacetic acid. The synthesized compound was recrystallized by slow evaporation of the saturated solution of ethanol and single crystal was selected for X-ray Diffraction study and was characterized by UV–Vis, FT-IR, 1H NMR spectroscopic techniques. A triclinic unit cell of C26H23N3O3S was diffracted for X-ray beam of wavelength 0.71075Å generated from Mo-Kα, data were solved by SHELXL-97 and molecular and packing diagram were determined by MERCURY, from which R value obtained was 0.0613.
| Item Type: | Article |
|---|---|
| Uncontrolled Keywords: | Crystal structure, Refinement, SHELXL- 97, Benzothiazole, DCC |
| Subjects: | B Life Science > Environmental Science |
| Divisions: | Department of > Environmental Science |
| Depositing User: | C Swapna Library Assistant |
| Date Deposited: | 14 Jun 2019 06:10 |
| Last Modified: | 14 Jun 2019 06:10 |
| URI: | http://eprints.uni-mysore.ac.in/id/eprint/3045 |
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