Synthesis, crystal structure, and characterization of (z)-2-(3-chlorophenyl)-n'-hydroxyacetamidine

Prabhuswamy, M. and Dinesha and Abdoh, M. M. M. and Pampa, K. J. and Kumar, S. M. and Nagaraja, G. K. and Lokanath, N. K. (2015) Synthesis, crystal structure, and characterization of (z)-2-(3-chlorophenyl)-n'-hydroxyacetamidine. MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 606 (1). pp. 189-198. ISSN 1563-5287

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Official URL: http://doi.org/10.1080/15421406.2014.905087

Abstract

The compound (Z)-2-(3-chlorophenyl)-N'-hydroxyacetamidine, (2) was synthesized and characterized by H-1 NMR, FT-IR, TGA, UV-Visible Spectra, and elemental analysis. Its molecular structure was solved by single-crystal X-ray diffraction method. The title molecule, C8H9ClN2O is crystallized in the monoclinic crystal system with the space group P2(1)/c and with unit cell parameters a = 8.7092(4) angstrom, b = 8.2370(4) angstrom, c = 12.5256(6) angstrom, beta = 102.252(3)degrees, and Z = 4. The molecular and crystal structure of the title molecule is stabilized by an intramolecular interaction of the type N-HcccO, and the intermolecular interactions of types N-HcccN and O-HcccN.

Item Type: Article
Subjects: B Life Science > Microbiology
D Physical Science > Physics
Divisions: Department of > Microbiology
Department of > Physics
Depositing User: Shrirekha N
Date Deposited: 17 Jun 2019 05:54
Last Modified: 17 Jun 2019 05:54
URI: http://eprints.uni-mysore.ac.in/id/eprint/2804

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