Synthesis, Characterization, Crystal, and Molecular Structure Analysis of 3,4-dihydro-6-(2-hydroxyphenyl)-5-nitro-4-phenylpyrimidin-2(1H)-one

Savant, M. M. and Gowda, L. B. and Anandalwar, S. M. and Prasad, J. S. and Shah, A. and Naliapara, Y. T. (2015) Synthesis, Characterization, Crystal, and Molecular Structure Analysis of 3,4-dihydro-6-(2-hydroxyphenyl)-5-nitro-4-phenylpyrimidin-2(1H)-one. MOLECULAR CRYSTALS AND LIQUID CRYSTALS, 609 (1). pp. 118-125. ISSN 1563-5287

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Official URL: https://doi.org/10.1080/15421406.2014.928425

Abstract

A novel nitro and 2-hydroxyphenyl functionalized pyrimidinone at C5 and C6, respectively, has been synthesized using 1-(2-hydroxyphenyl)-2-nitroethanone, benzaldehyde, urea, and etidronic acid as a catalyst is described. The synthesized compound characterized by spectroscopic techniques and finally confirmed by X-ray diffraction studies. The molecule crystallizes in the monoclinic crystal class in the space group P2(1)/c with cell parameters a = 11.1070(10)angstrom, b = 8.8210(4)angstrom, c = 15.1110(13)angstrom, beta = 106.193(2)degrees, and Z = 4. The pyrimidine ring adopts flattened boat conformation.

Item Type: Article
Subjects: D Physical Science > Physics
Divisions: Department of > Physics
Depositing User: Shrirekha N
Date Deposited: 13 Jun 2019 05:32
Last Modified: 13 Jun 2019 05:32
URI: http://eprints.uni-mysore.ac.in/id/eprint/2765

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