Keerthana, D. S. and Namratha, K. and Byrappa, K. and Yathirajan, H. S. (2015) Facile one-step fabrication of magnetite particles under mild hydrothermal conditions. JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 378. pp. 551-557. ISSN 1873-4766
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Hydrophilic magnetite particles for biological applications were synthesized by hydrothermal method in the presence of is-Glucose as both reducing and capping agent in a facile, one-step, low energy and environmentally friendly route. The role of D-Glucose as a reducing agent in the formation of magnetite particles under mild hydrothermal conditions has been investigated. The absence D-Glucose results in the formation of hematite. The magnetite particles synthesized were characterized using powder X-ray Diffraction (XRD), Fourier Transform infrared (FTIR) Spectroscopy, High Resolution Scanning Electron Microscopy (HR-SEM), Dynamic Light Scattering (DLS) and Vibrating Sample Magnetometery (VSM). The influence of the quantity of D-Glucose used and the reaction duration On the formation of magnetite were studied. DLS and HR-SEM results show that the size of the particles was in nano- to micron range. The antioxidant potency of the particles was confirmed using DPPH assay, where 2,2- Diphenyl-l-picrylhydrazyl was used as a source of free radicals. Hence the magnetite particles obtained could be considered for the use in various biological applications. (C) 2014 Elsevier B.V. All rights reserved
| Item Type: | Article |
|---|---|
| Subjects: | C Chemical Science > Chemistry D Physical Science > Material Science |
| Divisions: | Department of > Chemistry Department of > Material Science |
| Depositing User: | Users 19 not found. |
| Date Deposited: | 12 Jun 2019 10:30 |
| Last Modified: | 12 Jun 2019 10:30 |
| URI: | http://eprints.uni-mysore.ac.in/id/eprint/2762 |
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